No, he was squeezed by the hand and blood came out, but we never saw what happened to his body. Considering the ridiculous amount of blood anime characters tend of have, that's not convincing me that he was dead. After that he got smashed into the ground but then again that doesn't mean he was dead, people get smashed into walls and rocks and stuff all the time in that manga. He then got impaled by the arrow, but again, Naruto and most anime characters survive woulds like that all the time. He took fatal attacks after that, but that was after he had already activated the jutsu.